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Crystal Growth and Characterization Studies of a Zigzag 1D Sulfonated Coordination Polymer to Prepare Zinc Oxide Nanoparticles | ||
Journal of Sciences, Islamic Republic of Iran | ||
مقاله 4، دوره 34، شماره 1، خرداد 2023، صفحه 27-33 اصل مقاله (999.47 K) | ||
نوع مقاله: Original Paper | ||
شناسه دیجیتال (DOI): 10.22059/jsciences.2023.348173.1007754 | ||
نویسندگان | ||
shokoofeh Geranmayeh* 1؛ Faezeh Tabesh2؛ Alireza Abbasi2 | ||
11 Department of Physical Chemistry and Nanochemistry, Faculty of Chemistry, Alzahra University, Tehran, Islamic Republic of Iran | ||
22 School of Chemistry, College of Science, University of Tehran, Tehran, Islamic Republic of Iran | ||
چکیده | ||
Single crystals of a new coordination polymer, {[Zn(2,2’-bipyridine)(H2O)2(1,5-NDS)].2H2O}, where 1,5-NDS is 1,5-naphthalenedisulfonate ion, have been successfully grown under hydrothermal conditions. The as-synthesised coordination polymer was characterised by X-ray Diffraction analysis which shows that the metal centres have been linked by 1,5-NDS linkers and then the structure has extended in a 1D chain. Moreover, the compound was studied using thermogravimetric analysis (TGA) to check its thermal stability and IR spectroscopy. The prepared compound was a good candidate as a precursor to prepare ZnO nanoparticles. ZnO nanoparticles which were achieved after calcinating the compound, were characterized by Scanning Electron Microscopy (SEM) and PXRD. | ||
کلیدواژهها | ||
Coordination polymer؛ Nanoparticles؛ Single crystal؛ Sulfonated | ||
آمار تعداد مشاهده مقاله: 145 تعداد دریافت فایل اصل مقاله: 207 |