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Mirdehghan Ashkezari, Seyed Mohsen, Bahmanyar, H., Azizpour, Hedayat, Mohammadi, Mohammad, Najafipour, Iman. (1400). Investigation of Operating Parameters on Ultrasound-Assisted Extraction of Anethole in Fennel Essential Oil. , 55(2), 339-351. doi: 10.22059/jchpe.2021.325123.1352
Seyed Mohsen Mirdehghan Ashkezari; H. Bahmanyar; Hedayat Azizpour; Mohammad Mohammadi; Iman Najafipour. "Investigation of Operating Parameters on Ultrasound-Assisted Extraction of Anethole in Fennel Essential Oil". , 55, 2, 1400, 339-351. doi: 10.22059/jchpe.2021.325123.1352
Mirdehghan Ashkezari, Seyed Mohsen, Bahmanyar, H., Azizpour, Hedayat, Mohammadi, Mohammad, Najafipour, Iman. (1400). 'Investigation of Operating Parameters on Ultrasound-Assisted Extraction of Anethole in Fennel Essential Oil', , 55(2), pp. 339-351. doi: 10.22059/jchpe.2021.325123.1352
Mirdehghan Ashkezari, Seyed Mohsen, Bahmanyar, H., Azizpour, Hedayat, Mohammadi, Mohammad, Najafipour, Iman. Investigation of Operating Parameters on Ultrasound-Assisted Extraction of Anethole in Fennel Essential Oil. , 1400; 55(2): 339-351. doi: 10.22059/jchpe.2021.325123.1352

Investigation of Operating Parameters on Ultrasound-Assisted Extraction of Anethole in Fennel Essential Oil

Journal of Chemical and Petroleum Engineering
مقاله 9، دوره 55، شماره 2، اسفند 2021، صفحه 339-351    اصل مقاله (1.21 M)
نوع مقاله: Research Paper
شناسه دیجیتال (DOI): 10.22059/jchpe.2021.325123.1352
نویسندگان
Seyed Mohsen Mirdehghan Ashkezari1؛ H. Bahmanyar* 1؛ Hedayat Azizpour* 1؛ Mohammad Mohammadi1؛ Iman Najafipour2
1Surface Phenomenon and Liquid-Liquid Extraction Research Lab, School of Chemical Engineering, College of Engineering, University of Tehran, Tehran, Iran
2Fouman Faculty of Engineering, College of Engineering, University of Tehran, Tehran, Iran
چکیده
In this paper, the operational impact of three parameters including power of ultrasonic apparatus, size of fennel seeds and experiment time on the extraction yield of Anethole, which is the main considerable component in fennel essential oil and its concentration have been studied through Ultrasound-Assisted Extraction. The ultrasonic extraction of oil from fennel seeds using a solution of 70% water-ethanol was studied at different particle sizes, different ultrasonic powers and three different levels of time. The most effective parameter was particle size, while the experiment time had the least impact on both the efficiency and Anethole concentration as well. As a result, compared to Soxhlet method, the ultrasonic-assisted extraction was more efficient. In this experiment, eighteen constituents were identified for fennel seeds using GC–MS. The major components were Anethole (78.12%), Fenchone (8.81%), Limonene (4.39%), and Estragole (4.52%). Furthermore, the analysis of two quadratic models using the Box-Behnken design (BBD) indicated that the quadratic polynomial model can be applied for estimating the Anethole extraction yield as well as Anethole concentration.
کلیدواژه‌ها
Fennel؛ Anethole؛ Soxhlet؛ Ultrasound-Assisted؛ Extraction
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