سامانه پشتیبانی خدمات اطلاعات

  اخبار و اعلانات

 آمار

تعداد نشریات158
تعداد شماره‌ها6,225
تعداد مقالات67,685
تعداد مشاهده مقاله114,973,512
تعداد دریافت فایل اصل مقاله89,645,753
Shabani, Mahsa, Faraji, Ghader. (1399). Processing and Characterization of Natural Hydroxyapatite Powder from Bovine Bone. , 53(2), 204-209. doi: 10.22059/jufgnsm.2020.02.12
Mahsa Shabani; Ghader Faraji. "Processing and Characterization of Natural Hydroxyapatite Powder from Bovine Bone". , 53, 2, 1399, 204-209. doi: 10.22059/jufgnsm.2020.02.12
Shabani, Mahsa, Faraji, Ghader. (1399). 'Processing and Characterization of Natural Hydroxyapatite Powder from Bovine Bone', , 53(2), pp. 204-209. doi: 10.22059/jufgnsm.2020.02.12
Shabani, Mahsa, Faraji, Ghader. Processing and Characterization of Natural Hydroxyapatite Powder from Bovine Bone. , 1399; 53(2): 204-209. doi: 10.22059/jufgnsm.2020.02.12

Processing and Characterization of Natural Hydroxyapatite Powder from Bovine Bone

Journal of Ultrafine Grained and Nanostructured Materials
دوره 53، شماره 2، اسفند 2020، صفحه 204-209    اصل مقاله (1.16 M)
نوع مقاله: Research Paper
شناسه دیجیتال (DOI): 10.22059/jufgnsm.2020.02.12
نویسندگان
Mahsa Shabani؛ Ghader Faraji*
School of Mechanical Engineering, College of Engineering, University of Tehran, Tehran, Iran.
چکیده
In this paper, hydroxyapatite powder is produced via annealing of Bovine bone. The as received bovine bone was annealed at three different temperatures of 400 ℃, 700 ℃, and 1000 ℃ after a primary preparation stage. The powders obtained from annealed bovine bone were analyzed and characterized by Scanning Electron Microscope (SEM), X-Ray Diffraction (XRD), and Energy-Dispersive X-ray (EDX) spectroscopy. The XRD analysis showed that the annealed bone at 1000℃ is pure hydroxyapatite, at 700 ℃, it is mostly hydroxyapatite, and at 400℃, there are not enough hydroxyapatite crystals. The morphology of the samples was analyzed by SEM. It was observed that the bone annealed at 1000 ℃ exhibits human bone-like matrix particle shapes while at 400 ℃, and 700 ℃, the irregular shape exists. EDX analysis showed that Ca, P, C, and O were detected in the samples, while Ca and P were the major components. Also, the Ca/P ratios were more than 1.67, which is the ratio of stoichiometric hydroxyapatite.
کلیدواژه‌ها
Hydroxyapatite؛ Bovine bone؛ Annealing؛ Characterization
مراجع

1. Yılmaz P, öztürk Er E, Bakırdere S, ülgen K, özbek B. Application of supercritical gel drying method on fabrication of mechanically improved and biologically safe three-component scaffold composed of graphene oxide/chitosan/hydroxyapatite and characterization studies. Journal of Materials Research and Technology. 2019;8(6):5201-16.

2. Reshadi F, Faraji G, Baniassadi M, Tajeddini M. Surface modification of severe plastically deformed ultrafine grained pure titanium by plasma electrolytic oxidation. Surface and Coatings Technology. 2017;316:113-21.

3. Zhang J, Jia J, Kim JP, Shen H, Yang F, Zhang Q, et al. Ionic Colloidal Molding as a Biomimetic Scaffolding Strategy for Uniform Bone Tissue Regeneration. Advanced Materials. 2017;29(17):1605546.

4. Reshadi F, Faraji G, Moghtaderi H, Faghihi S. Surface and Bulk Modification of Titanium Grade 2 Substrates for Enhanced Biological Activity. JOM. 2020;72(2):721-9.

5. Teh SJ, Lai CW. Carbon nanotubes for dental implants. Applications of Nanocomposite Materials in Dentistry: Elsevier; 2018. p. 93-105.

6. Goodacre CJ, Bernal G, Rungcharassaeng K, Kan JYK. Clinical complications with implants and implant prostheses. The Journal of Prosthetic Dentistry. 2003;90(2):121-32.

7. Herberts P, Malchau H. Long-term registration has improved the quality of hip replacement: A review of the Swedish THR Register comparing 160,000 cases. Acta Orthopaedica Scandinavica. 2000;71(2):111-21.

8. Hemmerl  J,  n ag A, Ert rk S. Ultrastructural features of the bone response to a plasma-sprayed hydroxyapatite coating in sheep. Journal of Biomedical Materials Research. 1997;36(3):418-25.

9. Sun L, Berndt CC, Gross KA, Kucuk A. Material fundamentals and clinical performance of plasma-sprayed hydroxyapatite coatings: A review. Journal of Biomedical Materials Research. 2001;58(5):570-92.

10. Alagarsamy K, Vishwakarma V, Kaliaraj GS, Viswanathan K, Chavali M. Implant application of bioactive nano-hydroxyapatite powders—a comparative study. Materials Research Express. 2018;5(1):015405.

11. Mohd Pu'ad NAS, Koshy P, Abdullah HZ, Idris MI, Lee TC. Syntheses of hydroxyapatite from natural sources. Heliyon. 2019;5(5):e01588-e.

12. Pramanik S, Hanif ASM, Pingguan-Murphy B, Abu Osman NA. Morphological Change of Heat Treated Bovine Bone: A Comparative Study. Materials (Basel). 2013;6(1):65-75.

13. Ooi CY, Hamdi M, Ramesh S. Properties of hydroxyapatite produced by annealing of bovine bone. Ceramics International. 2007;33(7):1171-7.

14. Gergely G, Wéber F, Lukács I, Tóth AL, Horváth ZE, Mihály J, et al. Preparation and characterization of hydroxyapatite from eggshell. Ceramics International. 2010;36(2):803-6.

15. Joschek S, Nies B, Krotz R, Göpferich A. Chemical and physicochemical characterization of porous hydroxyapatite ceramics made of natural bone. Biomaterials. 2000;21(16):1645-58.

16. Zhou J, Zhang X, Chen J, Zeng S, De Groot K. High temperature characteristics of synthetic hydroxyapatite. Journal of Materials Science: Materials in Medicine. 1993;4(1):83-5.

17. Lamsihar Manalu J, Soegijono B, Indrani DJ. Characterization of Hydroxyapatite Derived from Bovine Bone. Asian J Appl Sci 2015;03:2321-0893.

18. Asaduzzaman SM. Extraction of Hydroxyapatite from Bovine and Human Cortical Bone by Thermal Decomposition and Effect of Gamma Radiation: A Comparative Study. International Journal of Complementary & Alternative Medicine. 2017;8(3).

19. Prevéy PS. X-Ray Diffraction Characterization of Crystallinity and Phase Composition in Plasma-Sprayed Hydroxyapatite Coatings. Journal of Thermal Spray Technology. 2000;9(3):369-76.

20. Sobczak-Kupiec A, Malina D, Kijkowska R, Wzorek Z. Comparative study of hydroxyapatite prepared by the authors with selected commercially available ceramics. Digest Journal of Nanomaterials and Biostructures. 2012 Jan 1;7(1):385-91.

21. Khoo W, Nor FM, Ardhyananta H, Kurniawan D. Preparation of Natural Hydroxyapatite from Bovine Femur Bones Using Calcination at Various Temperatures. Procedia Manufacturing. 2015;2:196-201.

22. Landi E, Tampieri A, Celotti G, Sprio S. Densification behaviour and mechanisms of synthetic hydroxyapatites. Journal of the European Ceramic Society. 2000;20(14-15):2377-87.

23. Pang YX, Bao X. Influence of temperature, ripening time and calcination on the morphology and crystallinity of hydroxyapatite nanoparticles. Journal of the European Ceramic Society. 2003;23(10):1697-704.

24. Murugan R, Rao KP, Kumar TSS. Heat-deproteinated xenogeneic bone from slaughterhouse waste: Physico-chemical properties. Bulletin of Materials Science. 2003;26(5):523-8.

25. Bano N, Adzila S, Jikan SS, Basri H, Kanasan N. Extraction of Biological Apatite from Cow Bone at Different Calcination Temperatures: A Comparative Study. Key Engineering Materials. 2019;796:46-52.

26. Doostmohammadi A, Monshi A, Fathi MH, Braissant O. A comparative physico-chemical study of bioactive glass and bone-derived hydroxyapatite. Ceramics International. 2011;37(5):1601-7.

 

آمار
تعداد مشاهده مقاله: 693
تعداد دریافت فایل اصل مقاله: 497


سامانه مدیریت نشریات علمی. قدرت گرفته از سیناوب