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SYNTHESIS, CHARACTERIZATION AND CATALYTIC BEHAVIOUR OF SPECIAL TYPE OF SILICO ALUMINO-PHOSPHATE WITH OPAL STRUCTURE | ||
| Journal of Sciences, Islamic Republic of Iran | ||
| مقاله 4، دوره 14، شماره 3، آذر 2003 اصل مقاله (122.91 K) | ||
| چکیده | ||
| In this study a special type of silicoaluminophosphate with opal structure (Opal-SAPO) was prepared under microwave condition using tetraethylorthosilicate (TEOS), triethanolamine (TEA), aluminiumisopropoxid and phosphoric acid 85%. The product was characterized by X-ray diffraction (XRD), thermogravimetric (TGA) and Fourier Infrared Spectroscopy (FTIR).The crystalline product showed a good activity and selectivity for regeneration of methylethylketone, benzaldehyde, and cyclohexanone from their semicarbazones derivatives. | ||
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