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. (1378). SYNTHESIS OF NORBORNENE FURYL ESTERS AND THEIR ENZYMATIC KINETIC RESOLUTION BY PIG LIVER ESTRASE (PLE). , 10(3), -.
. "SYNTHESIS OF NORBORNENE FURYL ESTERS AND THEIR ENZYMATIC KINETIC RESOLUTION BY PIG LIVER ESTRASE (PLE)". , 10, 3, 1378, -.
. (1378). 'SYNTHESIS OF NORBORNENE FURYL ESTERS AND THEIR ENZYMATIC KINETIC RESOLUTION BY PIG LIVER ESTRASE (PLE)', , 10(3), pp. -.
. SYNTHESIS OF NORBORNENE FURYL ESTERS AND THEIR ENZYMATIC KINETIC RESOLUTION BY PIG LIVER ESTRASE (PLE). , 1378; 10(3): -.

SYNTHESIS OF NORBORNENE FURYL ESTERS AND THEIR ENZYMATIC KINETIC RESOLUTION BY PIG LIVER ESTRASE (PLE)

Journal of Sciences, Islamic Republic of Iran
مقاله 5، دوره 10، شماره 3، آذر 1999    اصل مقاله (445.88 K)
چکیده
The reaction of furylacrylic acid with cyclopentadiene in toluene gave the
expected Diels-Alder endo-and exo-adductsin -1 : 1 ratio. The adducts were separated
by iodolactonization method to provide 3-endo-(2'-furyl) bicyclo 12.2.11 hept-5-ene-
2-exo-carboxylic acid and 3-exo-(2'-fury1)bicyclo 12.2.11 hept-5-ene-2-endocarboxylic
acid. Esterification of these acids by MeI / HMPA gave the expected
methyl esters. Kinetic resolution of racemic endo- and exo-ester adducts by
PLE(phosphate buffer, pH, 8) provided the related optically active isomers
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