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. (1374). LITHIUM PERCHLORATE MEDIATED AMINATION REACTION OF ALDEHYDES: A NOVEL METHOD FOR SYNTHESIS OF N, N-DIALKYL-p-SILYLATED AMINES*. , 6(3), -.
. "LITHIUM PERCHLORATE MEDIATED AMINATION REACTION OF ALDEHYDES: A NOVEL METHOD FOR SYNTHESIS OF N, N-DIALKYL-p-SILYLATED AMINES*". , 6, 3, 1374, -.
. (1374). 'LITHIUM PERCHLORATE MEDIATED AMINATION REACTION OF ALDEHYDES: A NOVEL METHOD FOR SYNTHESIS OF N, N-DIALKYL-p-SILYLATED AMINES*', , 6(3), pp. -.
. LITHIUM PERCHLORATE MEDIATED AMINATION REACTION OF ALDEHYDES: A NOVEL METHOD FOR SYNTHESIS OF N, N-DIALKYL-p-SILYLATED AMINES*. , 1374; 6(3): -.

LITHIUM PERCHLORATE MEDIATED AMINATION REACTION OF ALDEHYDES: A NOVEL METHOD FOR SYNTHESIS OF N, N-DIALKYL-p-SILYLATED AMINES*

Journal of Sciences, Islamic Republic of Iran
مقاله 8، دوره 6، شماره 3، آبان 1995    اصل مقاله (193.67 K)
چکیده
P-Silylated N,N-dialkyl amines (5) were easily synthesized in good to
excellent yield from aldehydes (1), trimethylsilyldialkylamines (2), and
trimethylsilylmethylmagnesium chloride (4) in the presence of 5 M lithium
perchlorate solution in diethyl ether. The reaction Of (2) with aldehyde
proceeded smoothly in the LiCI0 , to give the imimum salt (3). Addition of
trimethylsilylmethylrnagnesium chloride (4) gave the desired product
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